In this lab, we conduct manual titration of fertilizer samples to determine soluble potash content, which is potassium. The ground fertilizer sample is dissolved in water and then reagents are added to it including sodium tetraphenylboron. We also add thiazole yellow as the endpoint indicator for titration. When the solution turns a faint pink color, then we can determine how much reagent was added and calculate potash.
Fertilizer samples are primarily examined for label claim verifications. The most common test requests are for: nitrogen, potash, phosphorus, and sulfur. Samples are received from our agency field inspectors who visit manufacturing and distribution facilities where feed and fertilizer are produced and/or sold.